Start with the page for The Robert and Deborah Aliber Persian Gallery and at the bottom you'll see all their other links, including one to their Catalog of Expedition Photographs. All these photographs were obviously taken before any extensive excavations or rebuilding had been done.
Here's some of the blurb on the gallery itself:
Hmm, I think I must try and get to Chicago one day as it's unlikely that I'll ever make it to Persepolis itself! (Yes, Marcus, I'm envious!)Roughly half of the Persian Gallery is devoted to artifacts from Persepolis, which thrived from approximately 520 B.C. until, in 331 B.C., Alexander the Great and his troops destroyed it. This portion of the gallery is dominated by a series of colossal sculptures made of polished, black limestone, including the head of a bull that once guarded the entrance to the Hundred-Column Hall and column capitals in the forms of bulls and composite creatures.
"We display plates from the royal tables, which were broken when Alexander destroyed the city. They were thrown against the walls and lay in the ruins until a team from the Oriental Institute recovered them," Wilson said.

Best regards,